ISO 18144:2003
Environmental tobacco smoke — Estimation of its contribution to respirable suspended particles — Method based on solanesol
ISO 18144:2003 specifies a method for the sampling and determination of respirable suspended particles (RSP) and for the estimation of the RSP fraction attributable to environmental tobacco smoke (ETS). This method is applicable to personal and area sampling. This method is compatible with the determinations of gravimetric RSP, ultraviolet particulate matter (UVPM) and fluorescent particulate matter (FPM), which are also used to estimate the contribution of ETS to RSP.
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TitlePage - Environmental tobacco smoke— Estimation of its contribution to respirable suspended ...
TableofContent - Contents Page
Foreword - Foreword
Introduction - Introduction
Scope - 1 Scope
NormativeReference - 2 Normative references
Clause1 - 4 Principle
Clause1 - 5 Limits and detection
Clause1 - 6 Reagents
UntitledSubclause2 - 6.1 Acetonitrile
UntitledSubclause2 - 6.2 Methanol
UntitledSubclause2 - 6.3 Solanesol
UntitledSubclause2 - 6.4 Helium
UntitledSubclause2 - 6.5 Solanesol standard solutions
UntitledSubclause3 - 6.5.1 Primary standard of solanesol
UntitledSubclause3 - 6.5.2 Secondary standard of solanesol
UntitledSubclause3 - 6.5.3 Tertiary standard of solanesol
UntitledSubclause3 - 6.5.4 Working standards of solanesol
Clause1 - 7 Apparatus
UntitledSubclause2 - 7.1 Sample collection system
UntitledSubclause3 - 7.1.1 Polytetrafluoroethylene (PTFE) membrane filter
UntitledSubclause3 - 7.1.2 Filter cassette
UntitledSubclause3 - 7.1.3 Bubble flowmeter
UntitledSubclause3 - 7.1.4 Personal sampling pump
UntitledSubclause3 - 7.1.5 Inertial impactor
UntitledSubclause3 - 7.1.6 Stopcock grease
UntitledSubclause2 - 7.2 Analytical system
UntitledSubclause3 - 7.2.1 High-performance liquid chromatography (HPLC) system
UntitledSubclause3 - 7.2.2 HPLC column
UntitledSubclause3 - 7.2.3 Guard cartridge column
UntitledSubclause3 - 7.2.4 Sample containers
UntitledSubclause2 - 7.3 Dispensing pipettes
UntitledSubclause2 - 7.4 Filter forceps
UntitledSubclause2 - 7.5 Wrist-action shaking device
UntitledSubclause2 - 7.6 One-mark pipettes
UntitledSubclause2 - 7.7 One-mark volumetric flasks
Clause1 - 8 Sampling procedure
Subclause2 - 8.1 Calibration of air pumping system
Subclause2 - 8.2 Sample collection
Clause1 - 9 Analytical procedure
Subclause2 - 9.1 Preparation of samples and blanks
Subclause2 - 9.2 Determination of solanesol
Subclause3 - 9.2.1 Setting up the apparatus
Subclause3 - 9.2.2 Analysis of samples and blanks
Subclause3 - 9.2.3 Constructing the solanesol calibration curve
Clause1 - 10 Expression of results
Subclause2 - 10.1 Calculation of solanesol contents
Subclause3 - 10.1.1 Solanesol content in the test solution
Subclause3 - 10.1.2 Solanesol content in the air
Subclause2 - 10.2 ETS-PM contribution to RSP as estimated by solanesol
Subclause3 - 10.2.1 Calculation of Sol-PM
Subclause3 - 10.2.2 Apportionment of RSP as estimated by Sol-PM
Clause1 - 11 Laboratory performance criteria and quality assurance
Clause1 - 12 Repeatability and reproducibility
Clause1 - 13 Test report
AnnexInformative - Laboratory performance criteria: Quality assurance measures
Clause1 - A.1 Standard operating procedures (SOPs)
UntitledSubclause2 - A.1.1 Users should generate SOPs describing and documenting the following...
UntitledSubclause2 - A.1.2 The SOPs should provide specific, step-by-step instructions and sho...
UntitledSubclause2 - A.1.3 Solanesol is typically not detected in sample blanks. Detectable qu...
UntitledSubclause2 - A.1.4 Periodically, wipe clean the surface of the inertial impactor and a...
UntitledSubclause2 - A.1.5 In the event that an initial sample result is above the calibration...
Clause1 - A.2 Calibration of personal sampling pumps
UntitledSubclause2 - A.2.1 Calibrate sampling pumps at the beginning and at the conclusion of ...
UntitledSubclause2 - A.2.2 Set the pump flow controller using a bubble flowmeter or mass flowm...
Clause1 - A.3 Method sensitivity, precision and linearity
UntitledSubclause2 - A.3.1 The sensitivity of this method is demonstrated by the detection lim...
UntitledSubclause2 - A.3.2 Determining repeatability and reproducibility ensures method precis...
UntitledSubclause2 - A.3.3 Non-linearity in the calibration curve may occur at concentrations ...
Clause1 - A.4 Method modification
UntitledSubclause2 - A.4.1 The sampling period described in this method may be extended beyond
UntitledSubclause2 - A.4.2 The flow rate of air through the filter may be increased up to
UntitledSubclause2 - A.4.3 The test solution resulting from the procedure described herein is ...
Clause1 - A.5 Safety
UntitledSubclause2 - A.5.1 If spilling of solvent or any of the reagents occurs, take quick an...
UntitledSubclause2 - A.5.2 When preparing standards, as with handling any chemicals, avoid con...
Bibliography - Bibliography
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TitlePage - Environmental tobacco smoke— Estimation of its contribution to respirable suspended ...
TableofContent - Contents Page
Foreword - Foreword
Introduction - Introduction
Scope - 1 Scope
NormativeReference - 2 Normative references
Clause1 - 4 Principle
Clause1 - 5 Limits and detection
Clause1 - 6 Reagents
UntitledSubclause2 - 6.1 Acetonitrile
UntitledSubclause2 - 6.2 Methanol
UntitledSubclause2 - 6.3 Solanesol
UntitledSubclause2 - 6.4 Helium
UntitledSubclause2 - 6.5 Solanesol standard solutions
UntitledSubclause3 - 6.5.1 Primary standard of solanesol
UntitledSubclause3 - 6.5.2 Secondary standard of solanesol
UntitledSubclause3 - 6.5.3 Tertiary standard of solanesol
UntitledSubclause3 - 6.5.4 Working standards of solanesol
Clause1 - 7 Apparatus
UntitledSubclause2 - 7.1 Sample collection system
UntitledSubclause3 - 7.1.1 Polytetrafluoroethylene (PTFE) membrane filter
UntitledSubclause3 - 7.1.2 Filter cassette
UntitledSubclause3 - 7.1.3 Bubble flowmeter
UntitledSubclause3 - 7.1.4 Personal sampling pump
UntitledSubclause3 - 7.1.5 Inertial impactor
UntitledSubclause3 - 7.1.6 Stopcock grease
UntitledSubclause2 - 7.2 Analytical system
UntitledSubclause3 - 7.2.1 High-performance liquid chromatography (HPLC) system
UntitledSubclause3 - 7.2.2 HPLC column
UntitledSubclause3 - 7.2.3 Guard cartridge column
UntitledSubclause3 - 7.2.4 Sample containers
UntitledSubclause2 - 7.3 Dispensing pipettes
UntitledSubclause2 - 7.4 Filter forceps
UntitledSubclause2 - 7.5 Wrist-action shaking device
UntitledSubclause2 - 7.6 One-mark pipettes
UntitledSubclause2 - 7.7 One-mark volumetric flasks
Clause1 - 8 Sampling procedure
Subclause2 - 8.1 Calibration of air pumping system
Subclause2 - 8.2 Sample collection
Clause1 - 9 Analytical procedure
Subclause2 - 9.1 Preparation of samples and blanks
Subclause2 - 9.2 Determination of solanesol
Subclause3 - 9.2.1 Setting up the apparatus
Subclause3 - 9.2.2 Analysis of samples and blanks
Subclause3 - 9.2.3 Constructing the solanesol calibration curve
Clause1 - 10 Expression of results
Subclause2 - 10.1 Calculation of solanesol contents
Subclause3 - 10.1.1 Solanesol content in the test solution
Subclause3 - 10.1.2 Solanesol content in the air
Subclause2 - 10.2 ETS-PM contribution to RSP as estimated by solanesol
Subclause3 - 10.2.1 Calculation of Sol-PM
Subclause3 - 10.2.2 Apportionment of RSP as estimated by Sol-PM
Clause1 - 11 Laboratory performance criteria and quality assurance
Clause1 - 12 Repeatability and reproducibility
Clause1 - 13 Test report
AnnexInformative - Laboratory performance criteria: Quality assurance measures
Clause1 - A.1 Standard operating procedures (SOPs)
UntitledSubclause2 - A.1.1 Users should generate SOPs describing and documenting the following...
UntitledSubclause2 - A.1.2 The SOPs should provide specific, step-by-step instructions and sho...
UntitledSubclause2 - A.1.3 Solanesol is typically not detected in sample blanks. Detectable qu...
UntitledSubclause2 - A.1.4 Periodically, wipe clean the surface of the inertial impactor and a...
UntitledSubclause2 - A.1.5 In the event that an initial sample result is above the calibration...
Clause1 - A.2 Calibration of personal sampling pumps
UntitledSubclause2 - A.2.1 Calibrate sampling pumps at the beginning and at the conclusion of ...
UntitledSubclause2 - A.2.2 Set the pump flow controller using a bubble flowmeter or mass flowm...
Clause1 - A.3 Method sensitivity, precision and linearity
UntitledSubclause2 - A.3.1 The sensitivity of this method is demonstrated by the detection lim...
UntitledSubclause2 - A.3.2 Determining repeatability and reproducibility ensures method precis...
UntitledSubclause2 - A.3.3 Non-linearity in the calibration curve may occur at concentrations ...
Clause1 - A.4 Method modification
UntitledSubclause2 - A.4.1 The sampling period described in this method may be extended beyond
UntitledSubclause2 - A.4.2 The flow rate of air through the filter may be increased up to
UntitledSubclause2 - A.4.3 The test solution resulting from the procedure described herein is ...
Clause1 - A.5 Safety
UntitledSubclause2 - A.5.1 If spilling of solvent or any of the reagents occurs, take quick an...
UntitledSubclause2 - A.5.2 When preparing standards, as with handling any chemicals, avoid con...
Bibliography - Bibliography