AS/NZS 3580.10.1:2016
Methods for sampling and analysis of ambient air - Method 10.1: Determination of particulate matter - Deposited matter - Gravimetric method
Provides regulatory and testing bodies with a Standard method for determining deposited matter that rapidly settles from the air. This revision includes a procedure for determining the mass deposition rate of metals present in the deposited matter.
AS/NZS 3580.10.1:2016 METHODS FOR SAMPLING AND ANALYSIS OF AMBIENT AIR - DETERMINATION OF PARTICULATE MATTER-DEPOSITED...
PREFACE
FOREWORD
METHOD
1 SCOPE
2 REFERENCED DOCUMENTS
3 DEFINITIONS
3.1 Ash
3.2 Combustible matter
3.3 Constant mass
3.4 Deposited matter
3.5 Insoluble matter
3.6 Soluble matter
3.7 Total solids
3.8 U95
4 PRINCIPLE
5 REAGENTS
5.1 General requirements
5.2 Copper sulfate solution
6 APPARATUS
6.1 Deposit gauge
6.2 Lid
6.3 Stand
6.4 Bird ring (optional)
6.5 Glassware
6.6 Filtration apparatus
6.7 Test sieve
6.8 Filter cutter
7 SAMPLING
7.1 Location
7.2 Positioning of the gauge
7.3 Period of exposure
7.4 Procedure
7.4.1 Preparation of deposit gauge
7.4.2 Gauge exchange
7.4.3 Storage
8 PROCEDURE FOR SAMPLE ANALYSIS
8.1 Determination of total solids
8.1.1 General
8.1.2 Procedure 1
8.1.3 Procedure 2
8.2 Determination of insoluble solids
8.2.1 General
8.2.2 Using Gooch crucibles with filter pads or silica crucibles with porous bases
8.2.3 Using Buchner funnel and filter pad
8.3 Determination of ash and combustible matter
8.3.1 General
8.3.2 Using Gooch crucibles with filter pads or silica crucibles with porous bases
8.3.3 Using Buchner funnel and filter pad
8.4 Determination of soluble solids
8.4.1 General
8.4.2 Using direct calculation
8.4.3 Using filtrate collected during the insoluble solids procedure
9 CALCULATION AND EXPRESSION OF RESULTS
9.1 Calculation
9.2 Expression of results
10 MEASUREMENT UNCERTAINTY
11 TEST REPORT
APPENDIX A - DETERMINATION OF DEPOSITION RATES OF METALS PRESENT IN DEPOSITED MATTER
A1 SCOPE
A2 PROCEDURE FOR METALS DEPOSITION ANALYSIS
A2.1 General
A2.2 Determination of insoluble metals
A2.3 Determination of soluble metals
A3 CALCULATION AND EXPRESSION OF RESULTS
A3.1 Calculation
A3.2 Expression of results
A4 MEASUREMENT UNCERTAINTY
A5 TEST REPORT
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References
Methods for sampling and analysis of ambient air - Part 9.15: Determination of suspended particulate matter - Particulate metals high or low volume sampler gravimetric collection - Inductively coupled plasma (ICP) spectrometric method
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AS/NZS 3580.10.1:2016 METHODS FOR SAMPLING AND ANALYSIS OF AMBIENT AIR - DETERMINATION OF PARTICULATE MATTER-DEPOSITED...
PREFACE
FOREWORD
METHOD
1 SCOPE
2 REFERENCED DOCUMENTS
3 DEFINITIONS
3.1 Ash
3.2 Combustible matter
3.3 Constant mass
3.4 Deposited matter
3.5 Insoluble matter
3.6 Soluble matter
3.7 Total solids
3.8 U95
4 PRINCIPLE
5 REAGENTS
5.1 General requirements
5.2 Copper sulfate solution
6 APPARATUS
6.1 Deposit gauge
6.2 Lid
6.3 Stand
6.4 Bird ring (optional)
6.5 Glassware
6.6 Filtration apparatus
6.7 Test sieve
6.8 Filter cutter
7 SAMPLING
7.1 Location
7.2 Positioning of the gauge
7.3 Period of exposure
7.4 Procedure
7.4.1 Preparation of deposit gauge
7.4.2 Gauge exchange
7.4.3 Storage
8 PROCEDURE FOR SAMPLE ANALYSIS
8.1 Determination of total solids
8.1.1 General
8.1.2 Procedure 1
8.1.3 Procedure 2
8.2 Determination of insoluble solids
8.2.1 General
8.2.2 Using Gooch crucibles with filter pads or silica crucibles with porous bases
8.2.3 Using Buchner funnel and filter pad
8.3 Determination of ash and combustible matter
8.3.1 General
8.3.2 Using Gooch crucibles with filter pads or silica crucibles with porous bases
8.3.3 Using Buchner funnel and filter pad
8.4 Determination of soluble solids
8.4.1 General
8.4.2 Using direct calculation
8.4.3 Using filtrate collected during the insoluble solids procedure
9 CALCULATION AND EXPRESSION OF RESULTS
9.1 Calculation
9.2 Expression of results
10 MEASUREMENT UNCERTAINTY
11 TEST REPORT
APPENDIX A - DETERMINATION OF DEPOSITION RATES OF METALS PRESENT IN DEPOSITED MATTER
A1 SCOPE
A2 PROCEDURE FOR METALS DEPOSITION ANALYSIS
A2.1 General
A2.2 Determination of insoluble metals
A2.3 Determination of soluble metals
A3 CALCULATION AND EXPRESSION OF RESULTS
A3.1 Calculation
A3.2 Expression of results
A4 MEASUREMENT UNCERTAINTY
A5 TEST REPORT