ISO 15366-2:2014
Nuclear fuel technology — Chemical separation and purification of uranium and plutonium in nitric acid solutions for isotopic and isotopic dilution analysis by solvent extraction chromatography — Part 2: Samples containing plutonium and uranium in the nan
ISO 15366-2:2014 describes procedures to chemically separate and purify uranium and plutonium in dissolved solutions of irradiated light water reactor fuels and in samples of high active liquid waste of spent fuel reprocessing plants, prior to their isotopic analysis by e.g. mass spectrometric method or alpha spectrometry. ISO 15366-2:2014 describes a slightly different separation technique from ISO 15366-1, based on the same chemistry, using smaller columns, different support material and special purification steps, applicable to samples containing plutonium and uranium amounts in the nanogram range and below. The detection limits were found to be 500 pg plutonium and 500 pg uranium.
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Section sec_1
Section sec_2
Section sec_3
Section sec_3.1
Section sec_3.2
Section sec_3.3
Section sec_3.4
Section sec_3.5
Section sec_4
Section sec_4.1
Section sec_4.2
Section sec_4.3
Section sec_4.4
Section sec_4.5
Section sec_4.6
Section sec_4.7
Section sec_4.8
Section sec_4.9
Section sec_4.10
Section sec_4.11
Section sec_5
Section sec_5.1
Section sec_5.2
Section sec_5.3
Section sec_5.4
Section sec_5.5
Section sec_5.6
Section sec_5.7
Section sec_5.8
Section sec_5.9
Section sec_5.10
Section sec_5.11
Section sec_5.12
Section sec_5.13
Section sec_5.14
Section sec_5.15
Section sec_5.16
Section sec_5.17
Section sec_5.18
Section sec_5.19
Section sec_5.20
Section sec_5.21
Section sec_5.22
Section sec_5.23
Section sec_5.24
Section sec_5.25
Table tab_a
Figure fig_1
Section sec_6
Section sec_7
Section sec_7.1
Section sec_7.2
Section sec_8
Section sec_8.1
Section sec_8.2
Section sec_8.3
Annex sec_A
Annex sec_A.1
Annex sec_A.2
Annex sec_A.2.1
Annex sec_A.2.2
Annex sec_A.2.3
Annex sec_A.2.4
Annex sec_A.2.5
Annex sec_A.3
Annex sec_A.3.1
Annex sec_A.3.2
Annex sec_A.3.3
Annex sec_A.3.4
Annex sec_A.3.5
Annex sec_A.3.6
Annex sec_A.4
Annex sec_A.4.1
Annex sec_A.4.2
Annex sec_A.4.3
Annex sec_A.4.4
Annex sec_A.4.5
Annex sec_A.4.6
Annex sec_A.4.7
Annex sec_A.5
Annex sec_A.5.1
Annex sec_A.5.2
Annex sec_A.5.3
Annex sec_A.5.4
Table tab_b
Figure fig_A.1
Reference ref_1
Reference ref_2
Reference ref_3
Reference ref_4
Reference ref_5
Reference ref_6
Reference ref_7
Foreword
1 Scope
2 Principle of the method
3 Apparatus
4 Reagents
5 Procedure (see Figure 1)
6 Characteristics of the separation
7 Quality control
8 Interferences
Annex A (normative) Packing and conditioning of the chromatographic mini-columns as used in the ISO 15366‑2 procedure, loaded with an inert polyethylene support coated with tri-n-octyl-phosphine-oxide (TOPO)
Bibliography
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Section sec_1
Section sec_2
Section sec_3
Section sec_3.1
Section sec_3.2
Section sec_3.3
Section sec_3.4
Section sec_3.5
Section sec_4
Section sec_4.1
Section sec_4.2
Section sec_4.3
Section sec_4.4
Section sec_4.5
Section sec_4.6
Section sec_4.7
Section sec_4.8
Section sec_4.9
Section sec_4.10
Section sec_4.11
Section sec_5
Section sec_5.1
Section sec_5.2
Section sec_5.3
Section sec_5.4
Section sec_5.5
Section sec_5.6
Section sec_5.7
Section sec_5.8
Section sec_5.9
Section sec_5.10
Section sec_5.11
Section sec_5.12
Section sec_5.13
Section sec_5.14
Section sec_5.15
Section sec_5.16
Section sec_5.17
Section sec_5.18
Section sec_5.19
Section sec_5.20
Section sec_5.21
Section sec_5.22
Section sec_5.23
Section sec_5.24
Section sec_5.25
Table tab_a
Figure fig_1
Section sec_6
Section sec_7
Section sec_7.1
Section sec_7.2
Section sec_8
Section sec_8.1
Section sec_8.2
Section sec_8.3
Annex sec_A
Annex sec_A.1
Annex sec_A.2
Annex sec_A.2.1
Annex sec_A.2.2
Annex sec_A.2.3
Annex sec_A.2.4
Annex sec_A.2.5
Annex sec_A.3
Annex sec_A.3.1
Annex sec_A.3.2
Annex sec_A.3.3
Annex sec_A.3.4
Annex sec_A.3.5
Annex sec_A.3.6
Annex sec_A.4
Annex sec_A.4.1
Annex sec_A.4.2
Annex sec_A.4.3
Annex sec_A.4.4
Annex sec_A.4.5
Annex sec_A.4.6
Annex sec_A.4.7
Annex sec_A.5
Annex sec_A.5.1
Annex sec_A.5.2
Annex sec_A.5.3
Annex sec_A.5.4
Table tab_b
Figure fig_A.1
Reference ref_1
Reference ref_2
Reference ref_3
Reference ref_4
Reference ref_5
Reference ref_6
Reference ref_7
Foreword
1 Scope
2 Principle of the method
3 Apparatus
4 Reagents
5 Procedure (see Figure 1)
6 Characteristics of the separation
7 Quality control
8 Interferences
Annex A (normative) Packing and conditioning of the chromatographic mini-columns as used in the ISO 15366‑2 procedure, loaded with an inert polyethylene support coated with tri-n-octyl-phosphine-oxide (TOPO)
Bibliography