ISO 15366-1:2014
Nuclear fuel technology — Chemical separation and purification of uranium and plutonium in nitric acid solutions for isotopic and isotopic dilution analysis by solvent extraction chromatography — Part 1: Samples containing plutonium in the microgram range
ISO 15366-1:2014 describes procedures to chemically separate and purify uranium and plutonium in dissolved solutions of irradiated light water reactor fuels and in samples of high active liquid waste of spent fuel reprocessing plants, prior to their isotopic analysis by e.g. mass spectrometric method or alpha spectrometry. ISO 15366-1:2014 describes a technique for the separation of uranium and plutonium in spent fuel type samples based on chromatographic method. The procedure applies to samples containing 1 μg to 150 μg Pu (IV) and (VI) and 0,1 mg to 2 mg U (IV) and (VI) in up to 2 ml of 3 mol·l-1 nitric acid solution. It is applicable to mixtures of uranium and plutonium in which the U/Pu-ratio can range from 0 up to 200.
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Section sec_1
Section sec_2
Section sec_3
Section sec_3.1
Section sec_3.2
Section sec_3.3
Section sec_3.4
Section sec_3.5
Section sec_4
Section sec_4.1
Section sec_4.2
Section sec_4.3
Section sec_4.4
Section sec_4.5
Section sec_4.6
Section sec_4.7
Section sec_4.8
Section sec_5
Section sec_5.1
Section sec_5.2
Section sec_5.3
Section sec_5.4
Section sec_5.5
Section sec_5.6
Section sec_5.7
Section sec_5.8
Section sec_5.9
Section sec_5.10
Section sec_5.11
Section sec_5.12
Section sec_5.13
Section sec_5.14
Section sec_5.15
Table tab_a
Figure fig_1
Section sec_6
Section sec_6.1
Section sec_6.2
Section sec_6.3
Section sec_6.4
Section sec_6.5
Section sec_6.6
Section sec_6.7
Section sec_7
Section sec_7.1
Section sec_7.2
Section sec_8
Section sec_8.1
Section sec_8.2
Section sec_8.3
Annex sec_A
Annex sec_A.1
Annex sec_A.2
Annex sec_A.2.1
Annex sec_A.2.2
Annex sec_A.2.3
Annex sec_A.2.4
Annex sec_A.2.5
Annex sec_A.3
Annex sec_A.3.1
Annex sec_A.3.2
Annex sec_A.3.3
Annex sec_A.3.4
Annex sec_A.3.5
Annex sec_A.3.6
Annex sec_A.4
Annex sec_A.4.1
Annex sec_A.4.2
Annex sec_A.4.3
Annex sec_A.4.4
Annex sec_A.4.5
Annex sec_A.4.6
Annex sec_A.4.7
Annex sec_A.4.8
Annex sec_A.4.9
Annex sec_A.5
Annex sec_A.5.1
Annex sec_A.5.2
Annex sec_A.5.3
Annex sec_A.5.4
Table tab_b
Figure fig_A.1
Reference ref_1
Reference ref_2
Reference ref_3
Reference ref_4
Reference ref_5
Reference ref_6
Foreword
1 Scope
2 Principle of the method
3 Apparatus
4 Reagents
5 Procedure (see Figure 1)
6 Characteristics of the separation
7 Quality control
8 Interferences
Annex A (normative) Packing and conditioning of the chromatographic columns as used in the ISO 15366 1 procedure, loaded with an inert silica support coated with tri-n-octyl-phosphine-oxide (TOPO)
Bibliography
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Section sec_1
Section sec_2
Section sec_3
Section sec_3.1
Section sec_3.2
Section sec_3.3
Section sec_3.4
Section sec_3.5
Section sec_4
Section sec_4.1
Section sec_4.2
Section sec_4.3
Section sec_4.4
Section sec_4.5
Section sec_4.6
Section sec_4.7
Section sec_4.8
Section sec_5
Section sec_5.1
Section sec_5.2
Section sec_5.3
Section sec_5.4
Section sec_5.5
Section sec_5.6
Section sec_5.7
Section sec_5.8
Section sec_5.9
Section sec_5.10
Section sec_5.11
Section sec_5.12
Section sec_5.13
Section sec_5.14
Section sec_5.15
Table tab_a
Figure fig_1
Section sec_6
Section sec_6.1
Section sec_6.2
Section sec_6.3
Section sec_6.4
Section sec_6.5
Section sec_6.6
Section sec_6.7
Section sec_7
Section sec_7.1
Section sec_7.2
Section sec_8
Section sec_8.1
Section sec_8.2
Section sec_8.3
Annex sec_A
Annex sec_A.1
Annex sec_A.2
Annex sec_A.2.1
Annex sec_A.2.2
Annex sec_A.2.3
Annex sec_A.2.4
Annex sec_A.2.5
Annex sec_A.3
Annex sec_A.3.1
Annex sec_A.3.2
Annex sec_A.3.3
Annex sec_A.3.4
Annex sec_A.3.5
Annex sec_A.3.6
Annex sec_A.4
Annex sec_A.4.1
Annex sec_A.4.2
Annex sec_A.4.3
Annex sec_A.4.4
Annex sec_A.4.5
Annex sec_A.4.6
Annex sec_A.4.7
Annex sec_A.4.8
Annex sec_A.4.9
Annex sec_A.5
Annex sec_A.5.1
Annex sec_A.5.2
Annex sec_A.5.3
Annex sec_A.5.4
Table tab_b
Figure fig_A.1
Reference ref_1
Reference ref_2
Reference ref_3
Reference ref_4
Reference ref_5
Reference ref_6
Foreword
1 Scope
2 Principle of the method
3 Apparatus
4 Reagents
5 Procedure (see Figure 1)
6 Characteristics of the separation
7 Quality control
8 Interferences
Annex A (normative) Packing and conditioning of the chromatographic columns as used in the ISO 15366 1 procedure, loaded with an inert silica support coated with tri-n-octyl-phosphine-oxide (TOPO)
Bibliography