ISO 5667-14:2014
Water quality — Sampling — Part 14: Guidance on quality assurance and quality control of environmental water sampling and handling
ISO 5667-14:2014 provides guidance on the selection and use of various quality assurance and quality control techniques relating to the manual sampling of surface, potable, waste, marine and ground waters.
NOTE The general principles outlined in this part of ISO 5667 might, in some circumstances, be applicable to sludge and sediment sampling.
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Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Sources of sampling error
5 Sampling quality
5.1 General
5.2 Technical and personnel requirements
5.3 Sampling manual
5.4 Training of sampling staff
6 Strategy and organization
6.1 Time, duration and frequency of sampling
6.2 Sampling collection locations
7 Sample collection and handling
7.1 Equipment and vehicle check prior to carrying out a sampling programme
7.2 Preparation for sampling on-site
7.3 Field measurements
7.4 Taking the samples
8 Sample identification
9 Field sample protocol
10 Transport and storage of samples
11 Sampling quality control techniques
11.1 General
11.2 Replicate quality control samples
11.3 Field blank samples
11.4 Rinsing of equipment (sampling containers)
11.5 Filtration recovery
11.6 Technique 1 — Spiked samples
11.7 Technique 2 — Spiked environmental samples
12 Analysis and interpretation of quality control data
12.1 Shewhart control charts
12.2 Construction of duplicate control charts
13 Independent audits
Annex A (informative) Common sources of sampling error[7]
Annex B (informative) Control charts
Annex C (informative) Sub-sampling using a homogenizer
Bibliography
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Foreword
Introduction
1 Scope
2 Normative references
3 Terms and definitions
4 Sources of sampling error
5 Sampling quality
5.1 General
5.2 Technical and personnel requirements
5.3 Sampling manual
5.4 Training of sampling staff
6 Strategy and organization
6.1 Time, duration and frequency of sampling
6.2 Sampling collection locations
7 Sample collection and handling
7.1 Equipment and vehicle check prior to carrying out a sampling programme
7.2 Preparation for sampling on-site
7.3 Field measurements
7.4 Taking the samples
8 Sample identification
9 Field sample protocol
10 Transport and storage of samples
11 Sampling quality control techniques
11.1 General
11.2 Replicate quality control samples
11.3 Field blank samples
11.4 Rinsing of equipment (sampling containers)
11.5 Filtration recovery
11.6 Technique 1 — Spiked samples
11.7 Technique 2 — Spiked environmental samples
12 Analysis and interpretation of quality control data
12.1 Shewhart control charts
12.2 Construction of duplicate control charts
13 Independent audits
Annex A (informative) Common sources of sampling error[7]
Annex B (informative) Control charts
Annex C (informative) Sub-sampling using a homogenizer
Bibliography