ISO 19613:2018
Fine ceramics (advanced ceramics, advanced technical ceramics) — Measurement of viscosity of ceramic slurry by use of a rotational viscometer
ISO 19613:2018 specifies a method for measurement of the viscosity of a ceramic slurry using a rotational viscometer.
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Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
4.1 Rotational viscometer with defined shear rate
4.2 Single cylinder viscometer
5 Apparatus
5.1 General
5.2 Rotational viscometer with defined shear rate.
5.2.1 Measuring system
5.2.2 Basic capacity of the instrument
5.2.3 Installation of rotational viscometer
5.3 Single cylinder viscometer.
5.3.1 Main body of single cylinder viscometer
5.3.2 Spindle
5.4 Temperature-control device.
5.4.1 Thermostat
5.4.2 Thermometer
6 Calibration of the rotational viscometer
7 Measurement condition
7.1 Temperature
7.2 Selection of geometry and/or spindle (shear rate or angular velocity)
8 Pretreatment of the sample
8.1 General
8.2 Degassing
8.3 Mixing and dispersion by ultrasonication
9 Measurement procedure
9.1 Sampling
9.2 Measurement at fixed shear rate or angular velocity
9.3 Repeat
10 Expression of the results
11 Test report
Annex A (informative) Coaxial double cylinder system
Annex B (informative) Cone and plate system
Annex C (informative) Parallel plate system
Annex D (informative) Single cylinder viscometer
Bibliography
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Foreword
1 Scope
2 Normative references
3 Terms and definitions
4 Principle
4.1 Rotational viscometer with defined shear rate
4.2 Single cylinder viscometer
5 Apparatus
5.1 General
5.2 Rotational viscometer with defined shear rate.
5.2.1 Measuring system
5.2.2 Basic capacity of the instrument
5.2.3 Installation of rotational viscometer
5.3 Single cylinder viscometer.
5.3.1 Main body of single cylinder viscometer
5.3.2 Spindle
5.4 Temperature-control device.
5.4.1 Thermostat
5.4.2 Thermometer
6 Calibration of the rotational viscometer
7 Measurement condition
7.1 Temperature
7.2 Selection of geometry and/or spindle (shear rate or angular velocity)
8 Pretreatment of the sample
8.1 General
8.2 Degassing
8.3 Mixing and dispersion by ultrasonication
9 Measurement procedure
9.1 Sampling
9.2 Measurement at fixed shear rate or angular velocity
9.3 Repeat
10 Expression of the results
11 Test report
Annex A (informative) Coaxial double cylinder system
Annex B (informative) Cone and plate system
Annex C (informative) Parallel plate system
Annex D (informative) Single cylinder viscometer
Bibliography