ISO 13914:2013
Soil quality — Determination of dioxins and furans and dioxin-like polychlorinated biphenyls by gas chromatography with high-resolution mass selective detection (GC/HRMS)
ISO 13914:2013 specifies a method for quantitative determination of 17 2,3,7,8-chlorine substituted dibenzo-p-dioxins and dibenzofurans and dioxin-like polychlorinated biphenyls in sludge, treated biowaste, and soil using liquid column chromatographic clean-up methods and GC/HRMS.
| Get this standard | Prices exclude GST | |
|---|---|---|
| PDF ( Single user document) |
$118.26 NZD
|
|
| HardCopy |
$152.17 NZD
|
|
| Networkable PDF |
Price varies
|
Section sec_1
Table tab_1
Section sec_2
Section sec_3
Section sec_4
Section sec_5
Section sec_5.1
Section sec_5.2
Section sec_6
Section sec_6.1
Section sec_6.2
Section sec_6.2.1
Section sec_6.2.2
Section sec_6.2.3
Section sec_6.3
Section sec_6.3.1
Section sec_6.3.2
Section sec_6.3.3
Section sec_6.4
Section sec_6.4.1
Section sec_6.4.2
Section sec_6.4.3
Section sec_6.5
Section sec_6.5.1
Section sec_6.5.2
Section sec_6.5.3
Section sec_6.5.4
Section sec_6.6
Section sec_6.6.1
Section sec_6.6.2
Section sec_6.6.3
Section sec_6.6.4
Section sec_7
Section sec_7.1
Section sec_7.2
Section sec_8
Section sec_8.1
Section sec_8.2
Table tab_2
Section sec_8.3
Section sec_8.3.1
Section sec_8.3.2
Section sec_8.3.3
Section sec_8.3.4
Section sec_8.3.5
Section sec_8.3.6
Section sec_8.3.7
Section sec_8.4
Section sec_8.5
Section sec_9
Section sec_9.1
Section sec_9.2
Section sec_9.3
Table tab_3
Table tab_4
Section sec_9.4
Section sec_9.4.1
Table tab_5
Section sec_9.4.2
Section sec_9.4.3
Section sec_9.5
Section sec_9.5.1
Section sec_9.5.2
Section sec_9.5.3
Section sec_9.5.4
Section sec_9.5.5
Section sec_9.5.6
Section sec_9.5.7
Section sec_9.6
Section sec_9.6.1
Section sec_9.6.2
Section sec_9.6.3
Table tab_6
Section sec_9.7
Section sec_9.7.1
Section sec_9.7.2
Section sec_9.7.3
Section sec_9.7.4
Section sec_9.7.5
Section sec_9.7.5.1
Section sec_9.7.5.2
Section sec_10
Section sec_11
Annex sec_A
Table tab_A.1
Annex sec_B
Annex sec_B.1
Table tab_B.1
Annex sec_B.2
Table tab_B.2
Table tab_B.2___1
Annex sec_C
Annex sec_C.1
Annex sec_C.1.1
Annex sec_C.1.2
Annex sec_C.1.2.1
Annex sec_C.1.2.2
Annex sec_C.1.2.3
Annex sec_C.1.2.4
Annex sec_C.1.2.5
Annex sec_C.1.2.6
Annex sec_C.1.2.7
Annex sec_C.1.2.8
Annex sec_C.1.2.9
Annex sec_C.1.2.10
Annex sec_C.1.2.11
Annex sec_C.1.2.12
Annex sec_C.1.2.13
Annex sec_C.1.2.14
Annex sec_C.1.2.15
Annex sec_C.1.2.16
Annex sec_C.1.3
Annex sec_C.1.3.1
Table tab_C.1
Table tab_C.2
Annex sec_C.1.3.2
Annex sec_C.1.3.3
Annex sec_C.1.3.3.1
Figure fig_C.1
Annex sec_C.1.3.3.2
Annex sec_C.1.3.3.2.1
Annex sec_C.1.3.3.2.2
Annex sec_C.1.3.3.2.3
Annex sec_C.1.3.3.3
Annex sec_C.1.3.3.3.1
Annex sec_C.1.3.3.3.2
Annex sec_C.1.3.3.3.3
Annex sec_C.1.3.3.3.4
Annex sec_C.1.3.3.4
Annex sec_C.1.3.4
Annex sec_C.1.3.4.1
Annex sec_C.1.3.4.2
Annex sec_C.2
Table tab_C.3
Annex sec_D
Annex sec_D.1
Annex sec_D.1.1
Annex sec_D.1.2
Annex sec_D.1.3
Table tab_D.1
Table tab_D.2
Reference ref_1
Reference ref_2
Reference ref_3
Reference ref_4
Reference ref_5
Reference ref_6
Reference ref_7
Reference ref_8
Reference ref_9
Reference ref_10
Reference ref_11
Reference ref_12
Reference ref_13
Reference ref_14
Reference ref_15
Reference ref_16
Reference ref_17
Reference ref_18
Reference ref_19
Reference ref_20
Reference ref_21
Reference ref_22
Reference ref_23
Bibliography
Foreword
Introduction
1 Scope
2 Normative references
3 Abbreviated terms
4 Principle
5 Reagents
5.1 Chemicals
5.2 Standards
6 Apparatus and materials
6.1 General
6.2 Equipment for sample preparation
6.3 Soxhlet extractor
6.4 Clean-up apparatus
6.5 Concentration apparatus
6.6 Other equipment
7 Sample storage and sample pretreatment
7.1 Sample storage
7.2 Sample pretreatment
8 Extraction and clean-up
8.1 General
8.2 Extraction
8.3 Clean-up
8.4 Final concentration of cleaned sample extract
8.5 Addition of recovery standard
9 GC/HRMS analysis
9.1 General
9.2 Gas chromatographic analysis
9.3 Mass spectrometric detection
9.4 Minimum requirements for identification of PCDF/PCDD and PCB
9.5 Minimum requirements for quantification of PCDF/PCDD and PCB
9.6 Calibration of the GC/HRMS system
9.7 Quantification of GC/HRMS results
10 Precision
11 Test report
Annex A (informative) Toxic equivalent factors
Annex B (informative) Repeatability and reproducibility data
Annex C (informative) Examples of extraction and clean-up methods
Annex D (informative) Examples of operation of GC/HRMS determination
Bibliography
Keep me up-to-date
Register to receive notifications when updates are made to this standard.
Related Information
Similar Standards
-
BS 7755-3.1:1994
Soil quality. Chemical methods, Determination of dry matter and water content on a mass basis by a gravimetric method
-
BS 7755-3.11:1995
Soil quality. Chemical methods, Determination of water-soluble and acid-soluble sulfate
-
BS 7755-3.12:1996
Soil quality. Chemical methods, Determination of the potential cation exchange capacity and exchangeable cations using barium chloride solution buffered at pH = 8.1
-
BS 7755-3.13:1998
Soil quality. Chemical methods, Determination of cadmium, chromium, cobalt, copper, lead, manganese, nickel and zinc in aqua regia extracts of soil. Flame and electrothermal atomic absorption spectrometric methods
Section sec_1
Table tab_1
Section sec_2
Section sec_3
Section sec_4
Section sec_5
Section sec_5.1
Section sec_5.2
Section sec_6
Section sec_6.1
Section sec_6.2
Section sec_6.2.1
Section sec_6.2.2
Section sec_6.2.3
Section sec_6.3
Section sec_6.3.1
Section sec_6.3.2
Section sec_6.3.3
Section sec_6.4
Section sec_6.4.1
Section sec_6.4.2
Section sec_6.4.3
Section sec_6.5
Section sec_6.5.1
Section sec_6.5.2
Section sec_6.5.3
Section sec_6.5.4
Section sec_6.6
Section sec_6.6.1
Section sec_6.6.2
Section sec_6.6.3
Section sec_6.6.4
Section sec_7
Section sec_7.1
Section sec_7.2
Section sec_8
Section sec_8.1
Section sec_8.2
Table tab_2
Section sec_8.3
Section sec_8.3.1
Section sec_8.3.2
Section sec_8.3.3
Section sec_8.3.4
Section sec_8.3.5
Section sec_8.3.6
Section sec_8.3.7
Section sec_8.4
Section sec_8.5
Section sec_9
Section sec_9.1
Section sec_9.2
Section sec_9.3
Table tab_3
Table tab_4
Section sec_9.4
Section sec_9.4.1
Table tab_5
Section sec_9.4.2
Section sec_9.4.3
Section sec_9.5
Section sec_9.5.1
Section sec_9.5.2
Section sec_9.5.3
Section sec_9.5.4
Section sec_9.5.5
Section sec_9.5.6
Section sec_9.5.7
Section sec_9.6
Section sec_9.6.1
Section sec_9.6.2
Section sec_9.6.3
Table tab_6
Section sec_9.7
Section sec_9.7.1
Section sec_9.7.2
Section sec_9.7.3
Section sec_9.7.4
Section sec_9.7.5
Section sec_9.7.5.1
Section sec_9.7.5.2
Section sec_10
Section sec_11
Annex sec_A
Table tab_A.1
Annex sec_B
Annex sec_B.1
Table tab_B.1
Annex sec_B.2
Table tab_B.2
Table tab_B.2___1
Annex sec_C
Annex sec_C.1
Annex sec_C.1.1
Annex sec_C.1.2
Annex sec_C.1.2.1
Annex sec_C.1.2.2
Annex sec_C.1.2.3
Annex sec_C.1.2.4
Annex sec_C.1.2.5
Annex sec_C.1.2.6
Annex sec_C.1.2.7
Annex sec_C.1.2.8
Annex sec_C.1.2.9
Annex sec_C.1.2.10
Annex sec_C.1.2.11
Annex sec_C.1.2.12
Annex sec_C.1.2.13
Annex sec_C.1.2.14
Annex sec_C.1.2.15
Annex sec_C.1.2.16
Annex sec_C.1.3
Annex sec_C.1.3.1
Table tab_C.1
Table tab_C.2
Annex sec_C.1.3.2
Annex sec_C.1.3.3
Annex sec_C.1.3.3.1
Figure fig_C.1
Annex sec_C.1.3.3.2
Annex sec_C.1.3.3.2.1
Annex sec_C.1.3.3.2.2
Annex sec_C.1.3.3.2.3
Annex sec_C.1.3.3.3
Annex sec_C.1.3.3.3.1
Annex sec_C.1.3.3.3.2
Annex sec_C.1.3.3.3.3
Annex sec_C.1.3.3.3.4
Annex sec_C.1.3.3.4
Annex sec_C.1.3.4
Annex sec_C.1.3.4.1
Annex sec_C.1.3.4.2
Annex sec_C.2
Table tab_C.3
Annex sec_D
Annex sec_D.1
Annex sec_D.1.1
Annex sec_D.1.2
Annex sec_D.1.3
Table tab_D.1
Table tab_D.2
Reference ref_1
Reference ref_2
Reference ref_3
Reference ref_4
Reference ref_5
Reference ref_6
Reference ref_7
Reference ref_8
Reference ref_9
Reference ref_10
Reference ref_11
Reference ref_12
Reference ref_13
Reference ref_14
Reference ref_15
Reference ref_16
Reference ref_17
Reference ref_18
Reference ref_19
Reference ref_20
Reference ref_21
Reference ref_22
Reference ref_23
Bibliography
Foreword
Introduction
1 Scope
2 Normative references
3 Abbreviated terms
4 Principle
5 Reagents
5.1 Chemicals
5.2 Standards
6 Apparatus and materials
6.1 General
6.2 Equipment for sample preparation
6.3 Soxhlet extractor
6.4 Clean-up apparatus
6.5 Concentration apparatus
6.6 Other equipment
7 Sample storage and sample pretreatment
7.1 Sample storage
7.2 Sample pretreatment
8 Extraction and clean-up
8.1 General
8.2 Extraction
8.3 Clean-up
8.4 Final concentration of cleaned sample extract
8.5 Addition of recovery standard
9 GC/HRMS analysis
9.1 General
9.2 Gas chromatographic analysis
9.3 Mass spectrometric detection
9.4 Minimum requirements for identification of PCDF/PCDD and PCB
9.5 Minimum requirements for quantification of PCDF/PCDD and PCB
9.6 Calibration of the GC/HRMS system
9.7 Quantification of GC/HRMS results
10 Precision
11 Test report
Annex A (informative) Toxic equivalent factors
Annex B (informative) Repeatability and reproducibility data
Annex C (informative) Examples of extraction and clean-up methods
Annex D (informative) Examples of operation of GC/HRMS determination
Bibliography